πŸ“– Theory & Concepts β–Ό

Acid-Base Titration

Hβ‚‚Cβ‚‚Oβ‚„ + 2NaOH β†’ Naβ‚‚Cβ‚‚Oβ‚„ + 2Hβ‚‚O
Primary Standard: Oxalic acid (exact concentration known)
Secondary Standard: NaOH (standardized against primary)
Indicator: Phenolphthalein (colorless β†’ pink at endpoint)

Key Formulas

N₁V₁ = Nβ‚‚Vβ‚‚ (at equivalence point)
Normality = Molarity Γ— n-factor
Oxalic acid n-factor = 2 (dibasic)

Tips for Accuracy

  • β€’ Remove air bubbles from burette before starting
  • β€’ Rinse burette with NaOH before filling
  • β€’ Swirl flask continuously while adding titrant
Did you know? The word "titration" comes from the French word "titre" meaning "title" or "rank" - originally used to describe determining the purity of gold!

🎯 Objective

Determine the strength of NaOH solution by titrating against standard oxalic acid using phenolphthalein indicator.

Procedure

1. Prepare 0.1N oxalic acid
2. Fill burette with NaOH
3. Add indicator to flask
4. Titrate until pink color
5. Note burette reading

Theory

Hβ‚‚Cβ‚‚Oβ‚„ + 2NaOH β†’ Naβ‚‚Cβ‚‚Oβ‚„ + 2Hβ‚‚O
Endpoint
Colorless β†’ Pale Pink
Formula
N₁V₁ = Nβ‚‚Vβ‚‚
Initial Reading
0.0 mL
Current Reading
0.0 mL
Volume Used
0.0 mL
Burette (NaOH)
01020304050
20 mL Oxalic Acid (0.1N)
No indicator added

πŸ“Š Titration Readings

# Initial Final Vol
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Lab Notebook
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